A new approach to the rapid separation of isomeric compounds in a Silybum marianum extract using UHPLC core‐shell column with F5 stationary phase

No abstract is available for this paper.

• Publication year

  2017

• Venue

  Journal of Pharmaceutical and Biomedical Analysis

• Publication date

  2017-02-05

• Fields of study

  Medicine, Chemistry

• Identifiers
  DOI 10.1016/j.jpba.2016.11.042PMID 27915198
• External record

  Open on Semantic Scholar

• Source metadata

  Semantic Scholar, PubMed

• No claims are published for this paper.

• No concepts are published for this paper.

• Head-to-Head Comparison of Ultra-High-Performance Liquid Chromatography with Diode Array Detection versus Quantitative Nuclear Magnetic Resonance for the Quantitative Analysis of the Silymarin Complex in Silybum marianum Fruit Extracts.

  2016cited by this paper
• A new method for rapid determination of indole-3-carbinol and its condensation products in nutraceuticals using core-shell column chromatography method.

  2016cited by this paper
• Simultaneous analysis of eight vitamin E isomers in Moringa oleifera Lam. leaves by ultra performance convergence chromatography.

  2016cited by this paper
• A study of retention characteristics and quality control of nutraceuticals containing resveratrol and polydatin using fused-core column chromatography.

  2016cited by this paper
• A validated UHPLC-tandem mass spectrometry method for quantitative analysis of flavonolignans in milk thistle (Silybum marianum) extracts.

  2016cited by this paper
• A New Gas Chromatography Method for Quality Control of Methylsulfonylmethane Content in Multicomponent Dietary Supplements

  2014cited by this paper
• UPLC method for the determination of vitamin E homologues and derivatives in vegetable oils, margarines and supplement capsules using pentafluorophenyl column.

  2014cited by this paper
• Chromatographic separation of arsenic species with pentafluorophenyl column and application to rice.

  2014cited by this paper
• Preparatory separation of the silymarin flavonolignans by Sephadex LH-20 gel

  2014cited by this paper
• A New and Fast HPLC Method for Determination of Rutin, Troxerutin, Diosmin and Hesperidin in Food Supplements Using Fused-Core Column Technology

  2013cited by this paper
• A Fast HPLC Method for Determination of Vitamin E Acetate in Dietary Supplements Using Monolithic Column

  2013cited by this paper
• Applications of superficially porous particles: high speed, high efficiency or both?

  2012cited by this paper
• A sensitive LC-MS/MS assay for the simultaneous analysis of the major active components of silymarin in human plasma.

  2012cited by this paper
• Fast liquid chromatography: the domination of core-shell and very fine particles.

  2012cited by this paper
• Silymarin: A Review of its Clinical Properties in the Management of Hepatic Disorders

  2012cited by this paper
• Preparation and Evaluation of Silymarin β-cyclodextrin Molecular Inclusion Complexes

  2011cited by this paper
• Rapid separation and characterization of active flavonolignans of Silybum marianum by ultra-performance liquid chromatography coupled with electrospray tandem mass spectrometry.

  2010cited by this paper
• A novel rapid method for simultaneous determination of eight active compounds in silymarin using a reversed-phase UPLC-UV detector.

  2009cited by this paper
• Validated Optimized Method for Simultaneous Analysis of Active Silymarin Components and Dimethyl-4,4′-dimethoxy-5,6,5′,6′-dimethylene Dioxybiphenyl-2,2′-dicarboxylate in a Pharmaceutical Preparation by Use of a Monolithic Silica C18 Column

  2009cited by this paper
• Fluorocarbon stationary phases for liquid chromatography applications

  2008cited by this paper
• Gram-scale purification of flavonolignan diastereoisomers from Silybum marianum (Milk Thistle) extract in support of preclinical in vivo studies for prostate cancer chemoprevention.

  2007cited by this paper
• Analysis and comparison of active constituents in commercial standardized silymarin extracts by liquid chromatography-electrospray ionization mass spectrometry.

  2007cited by this paper
• Fused-core particle technology as an alternative to sub-2-microm particles to achieve high separation efficiency with low backpressure.

  2007cited by this paper
• Separation and characterization of silybin, isosilybin, silydianin and silychristin in milk thistle extract by liquid chromatography-electrospray tandem mass spectrometry.

  2006cited by this paper
• Milk thistle and prostate cancer: differential effects of pure flavonolignans from Silybum marianum on antiproliferative end points in human prostate carcinoma cells.

  2005cited by this paper
• Silymarin treatment of viral hepatitis: a systematic review

  2005cited by this paper
• Analysis of the active components of silymarin.

  2003cited by this paper
• Determination of active component in silymarin by RP-LC and LC/MS.

  2001cited by this paper
• Inhibition of human carcinoma cell growth and DNA synthesis by silibinin, an active constituent of milk thistle: comparison with silymarin.

  1999cited by this paper

• Sequential selective supercritical fluid extraction (S3FE) of triglycerides and flavonolignans from milk thistle (Silybum marianum L, Gaertn)

  2023cites this paper
• Estimation of the Controlled Release of Antioxidants from β-Cyclodextrin/Chamomile (Matricaria chamomilla L.) or Milk Thistle (Silybum marianum L.), Asteraceae, Hydrophilic Extract Complexes through the Fast and Cheap Spectrophotometric Technique

  2023cites this paper
• Detecting and Profiling of Milk Thistle Metabolites in Food Supplements: A Safety-Oriented Approach by Advanced Analytics

  2023cites this paper
• Validation of a High-Performance Liquid Chromatography with Photodiode Array Detection Method for the Separation and Quantification of Antioxidant and Skin Anti-Aging Flavonoids from Nelumbo nucifera Gaertn. Stamen Extract

  2022cites this paper
• Anthocyanins in Different Food Matrices: Recent Updates on Extraction, Purification and Analysis Techniques

  2022cites this paper
• Controlled release of silibinin in GelMA hydrogels inhibits inflammation by inducing M2-type macrophage polarization and promotes vascularization in vitro

  2022cites this paper
• Qualitative and quantitative analysis of opiate and related metabolites in human urine samples by UPLC-MS/MS

  2021cites this paper
• Development of a capillary electrophoresis method for the separation of flavonolignans in silymarin complex

  2021cites this paper
• Quantification of 2-aminothiazoline-4-carboxylic acid as a reliable marker of cyanide exposure using chemical derivatization followed by liquid chromatography-tandem mass spectrometry.

  2021cites this paper
• Silybins: Antiviral liver analeptics

  2021cites this paper
• Chirality Matters: Biological Activity of Optically Pure Silybin and Its Congeners

  2021cites this paper
• Simultaneous HPLC-DAD determination of seven intense sweeteners in foodstuffs and pharmaceuticals using a core-shell particle column

  2021cites this paper
• Liquid chromatography–drift tube ion mobility–mass spectrometry as a new challenging tool for the separation and characterization of silymarin flavonolignans

  2020cites this paper
• New challenge in the lipophilicity determination and separation of biologically active 16,17-secoesterone derivatives by HPLC – Use of pentafluorophenyl-propyl column

  2020cites this paper
• Silymarin compounds: Chemistry, innovative extraction techniques and synthesis

  2020cites this paper
• A coupled method of on-line solid phase extraction with the UHPLC‒MS/MS for detection of sulfonamides antibiotics residues in aquaculture.

  2020cites this paper
• Determination of levofloxacin, ciprofloxacin, moxifloxacin and gemifloxacin in urine and plasma by HPLC-FLD-DAD using pentafluorophenyl core-shell column: Application to drug monitoring.

  2020cites this paper
• Maceration-Mediated Liquid-Liquid Extraction and Reverse-Phase High-Performance Liquid Chromatography-Based Pragmatic Analysis of Silybins.

  2020cites this paper
• Presence of Mycotoxins in Milk Thistle (Silybum marianum) Food Supplements: A Review

  2020cites this paper
• Retention-directed and selectivity controlled chromatographic resolution: Rapid post-hoc analysis of DMPK samples to achieve high-throughput LC-MS separation.

  2020cites this paper
• The Chemical Constituents and Pharmacological Actions of Silybum Marianum

  2019cites this paper
• Rapid discrimination and quantification of isomeric flavonoid‐O‐diglycosides in Citrus paradisi cv. changshanhuyou by online extraction–quadrupole time‐of flight tandem mass spectrometry

  2019cites this paper
• A direct comparison of liquid chromatography-mass spectrometry with clinical routine testing immunoassay methods for the detection and quantification of thyroid hormones in blood serum

  2019cites this paper
• Complex Evaluation of Antioxidant Capacity of Milk Thistle Dietary Supplements

  2019cites this paper
• Single Laboratory Validation of a Quantitative Core Shell-Based LC Separation for the Evaluation of Silymarin Variability and Associated Antioxidant Activity of Pakistani Ecotypes of Milk Thistle (Silybum Marianum L.)

  2018cites this paper
• Natural Strategies to Improve Quality in Food Protection

  2018cites this paper
• Selective recognition and preliminary separation of hepatoprotective component silybin from milk thistle seeds by the prepared core–shell magnetic molecularly imprinted polymer

  2018cites this paper
• Využití HPLC v analýze nutraceutik s obsahem chlorogenových kyselin

  2018cites this paper
• Current trends in the analysis and quality control of food supplements based on plant extracts.

  2018cites this paper
• 3-Amino-5-pyridin-3-yl-1,2,4-triazole, a novel fluorescence probe for trace analysis of silymarin in bulk material, pharmaceutical dosage forms and human plasma: Further insights on reaction mechanism using computational molecular modeling and NMR spectroscopy.

  2018cites this paper
• A validated UHPLC method for the determination of caffeoylquinic and di‐caffeoylquinic acids in green coffee extracts using an RP‐Amide fused‐core column

  2018cites this paper
• Amino-5-pyridin-3-yl-1 , 2 , 4-triazole , a novel fl uorescence probe for trace analysis of silymarin in bulkmaterial , pharmaceutical dosage forms and human plasma : Further insights on reaction mechanism using computational molecular modeling and NMR spectroscopy

  2018cites this paper
• Revising Reverse-Phase Chromatographic Behavior for Efficient Differentiation of Both Positional and Geometrical Isomers of Dicaffeoylquinic Acids

  2018cites this paper
• A rapid, simple, and high‐throughput UPLC‐MS/MS method for simultaneous determination of bioactive constituents in Salvia miltiorrhiza with positive/negative ionization switching

  2018cites this paper
• Assessment of the Antioxidant Activity and Quality Attributes of Yogurt Enhanced with Wild Herbs Extracts

  2018cites this paper
• A UHPLC method for the rapid separation and quantification of anthocyanins in acai berry and dry blueberry extracts

  2017cites this paper
• The silymarin composition… and why does it matter???

  2017cites this paper