Separation of selected bioactive compounds from orange peel using the sequence of supercritical CO2 extraction and ultrasound solvent extraction: optimization of limonene and hesperidin content

ABSTRACT The orange peel (Citrus sinensis L.) from the variety Washington Navel was extracted by supercritical CO2 (SC-CO2) at different parameters. The extracts were analyzed by gas chromatography-mass spectrometry (GC-MS) and high-performance liquid chromatography (HPLC). Limonene predominance was found (up to 89%). The principal oxygenated monoterpenes were linalool, α-terpineol, decanal, and (E)-citral. Ultrasound-assisted extraction was performed on the remaining solid residue (after SC-CO2extraction) to obtain the extracts rich in hesperidin. The influence of different extraction parameters on hesperidin content (3.3–23.0 µg/mL) was determined. The prediction performance in optimizing the extraction yield of dominant compounds was studied by response surface methodology and artificial neural network.

• Publication year

  2019

• Venue

  Separation Science and Technology

• Publication date

  2019-07-26

• Fields of study

  Chemistry, Environmental Science

• Identifiers
  DOI 10.1080/01496395.2019.1647245
• External record

  Open on Semantic Scholar

• Source metadata

  Semantic Scholar

• No claims are published for this paper.

• No concepts are published for this paper.

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