In this paper, a pencil graphite electrode was pretreated using chronoamperometry technique in phosphate buffer solution (pH=7.0) for sensitive determination of quercetin. Oxidation of quercetin was investigated using pretreated pencil graphite electrode and anodic stripping differential pulse voltammetry. Under optimal conditions, the anodic current of quercetin exhibited linear response to its concentration in the range from 0.001 to 1.5 µmol/L with the limit of detection of 0.3·10-3 µmol/L. The proposed method was successfully applied for the determination of quercetin in cranberry and blackcurrant juices with recovery rate from 93.2 to 94.7%. Solid-phase extraction was found to be necessary prior to voltammetric determination of quercetin in fruit juice samples using pretreated pencil graphite electrode.
Sensitive Voltammetric Determination of Natural Flavonoid Quercetin on a Disposable Graphite Lead.
D. Vu,S. Žabčíková,L. Červenka,Bensu Ertek,Y. Dilgin
Published 2015 in Food Technology and Biotechnology
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- Publication year
2015
- Venue
Food Technology and Biotechnology
- Publication date
2015-12-28
- Fields of study
Medicine, Chemistry
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Semantic Scholar, PubMed
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