Accurate measurements of long-range heteronuclear coupling constants from homonuclear 2D NMR spectra of isotope-enriched proteins

No abstract is available for this paper.

• Publication year

  1989

• Venue

  Journal of Magnetic Resonance

• Publication date

  1989-03-01

• Fields of study

  Biology, Chemistry

• Identifiers
  DOI 10.1016/0022-2364(89)90183-2
• External record

  Open on Semantic Scholar

• Source metadata

  Semantic Scholar

• No claims are published for this paper.

• No concepts are published for this paper.

• Conformational properties of trans Ac-Asn-Pro-Tyr-NHMe and trans Ac-Tyr-Pro-Asn-NHMe in dimethylsulfoxide and in water determined by multinuclear n.m.r. spectroscopy.

  2009cited by this paper
• Novel three-dimensional NMR techniques for studies of peptides and biological macromolecules

  1987cited by this paper
• Stereospecific assignments of side-chain protons and characterization of torsion angles in Eglin c.

  1987cited by this paper
• Peptide conformations. 42. Conformation of side chains in peptides using heteronuclear coupling constants obtained by two-dimensional NMR spectroscopy

  1987cited by this paper
• The purification of fully active recombinant transforming growth factor alpha produced in Escherichia coli.

  1986cited by this paper
• Systematic application of high-resolution, phase-sensitive two-dimensional 1H-NMR techniques for the identification of the amino-acid-proton spin systems in proteins. Rabbit metallothionein-2.

  1985cited by this paper
• Product operator formalism for the description of NMR pulse experiments

  1984cited by this paper
• Human transforming growth factor-α: Precursor structure and expression in E. coli

  1984cited by this paper
• 113CD-1H spin-spin couplings in homonuclear 1H correlated spectroscopy of metallothionein. Identification of the cysteine 1H spin systems.

  1984cited by this paper
• TORSION ANGLES IN THE CYSTINE BRIDGE OF OXYTOCIN IN AQUEOUS SOLUTION. MEASUREMENTS OF CIRCUMJACENT VICINAL COUPLINGS BETWEEN PROTON, CARBON-13, AND NITROGEN-15

  1980cited by this paper
• 1H‐15N Spin–spin couplings in alumichrome

  1978cited by this paper
• Heteronuclear vicinal coupling constants and site-specific isotopic substitution in the investigation of rotational isomerism in leucine

  1978cited by this paper
• Spin—spin coupling and the conformational states of peptide systems

  1976cited by this paper
• The conformational dependence of vicinal 15N-C-C-H coupling constants in peptides

  1974cited by this paper
• Study of nitrogen-15-labeled amino acids and peptides by nuclear magnetic resonance spectroscopy.

  1973cited by this paper
• Nitrogen-15 magnetic resonance spectroscopy. X. Angular dependence of vicinal 15N-H coupling constants in amino acids.

  1970cited by this paper

• Conformational Studies on Two FtsZ Targeting Cyclic Peptides

  2019cites this paper
• Probing Protein-Protein Interactions Using Asymmetric Labeling and Carbonyl-Carbon Selective Heteronuclear NMR Spectroscopy

  2018cites this paper
• Stereoselective Deuteration in Aspartate, Asparagine, Lysine, and Methionine Amino Acid Residues Using Fumarate as a Carbon Source for Escherichia coli in D2O.

  2017cites this paper
• Determination of unresolved heteronuclear scalar coupling constants by J(up)-HSQMBC.

  2016cites this paper
• NMR Approaches to Functional Dynamics of Genetically Separated iGluR Domains

  2016cites this paper
• Ionotropic Glutamate Receptor Technologies

  2016cites this paper
• A toolbox of HSQC experiments for small molecules at high 13C‐enrichment. Artifact‐free, fully 13C‐homodecoupled and JCC‐encoding pulse sequences

  2013cites this paper
• Two-Dimensional Higher Quantum Correlation and Resolved Techniques for the Analyses of Complex 1H NMR Spectra of Scalar-Coupled Spins

  2013cites this paper
• Selective COSY‐J‐resolved‐HMBC, a new method for improving sensitivity of cross peaks of methine proton signals attached to a methyl group

  2012cites this paper
• Selective J‐resolved HMBC, an efficient method for measuring heteronuclear long‐range coupling constants

  2009cites this paper
• Structural determinants responsible for the thermostability of Sso7d and its single point mutants

  2007cites this paper
• Spin selective multiple quantum NMR for spectral simplification, determination of relative signs, and magnitudes of scalar couplings by spin state selection.

  2007cites this paper
• CHAPTER 7 – HETERONUCLEAR NMR EXPERIMENTS

  2007cites this paper
• Synthesis, NMR, and Conformational Studies of Fucoidan Fragments. VII.1 Influence of Length and 2,3‐Branching on the Conformational Behavior of Linear (1→3)‐Linked Oligofucoside Chains

  2005influential citation
• 2JC,H index: a nondestructive NMR method for differentiation of aldohexopyranosyl residues.

  2005cites this paper
• NMR of unfolded proteins

  2005cites this paper
• A generalized approach to automated NMR peak list editing: application to reduced dimensionality triple resonance spectra.

  2004cites this paper
• Cofactor‐Apoprotein Hydrogen Bonding in Oxidized and Fully Reduced Flavodoxin Monitored by Trans‐Hydrogen‐Bond Scalar Couplings

  2004cites this paper
• Methods for the Determination of Torsion Angle Restraints in Biomacromolecules

  2002cites this paper
• Pulse Sequences for Measuring Coupling Constants

  2002cites this paper
• Broadband composite spin-state-selective rotations for NMR spectroscopy on partially aligned molecules

  2001cites this paper
• NMR identification of local structural preferences in HIV‐1 protease tethered heterodimer in 6 M guanidine hydrochloride

  2001cites this paper
• Improved Measurement of 3J(Hαi, Ni+1) Coupling Constants in H2O Dissolved Proteins

  2001cites this paper
• Conformational Study of a Tetraacyl Biosynthetic Precursor of Lipid A by NMR

  2001cites this paper
• NMR structure of the channel‐former zervamicin IIB in isotropic solvents

  2000cites this paper
• Refinement of the protein backbone angle ψ in NMR structure calculations

  2000cites this paper
• Measurement of homonuclear (2)J-couplings from spin-state selective double-/zero-quantum two-dimensional NMR spectra.

  1999cites this paper
• HYPER: A hierarchical algorithm for automatic determination of protein dihedral-angle constraints and stereospecific CβH2 resonance assignments from NMR data

  1999cites this paper
• Accurate measurements of multiple-bond 13C-1H coupling constants from phase-sensitive 2D INEPT spectra.

  1999cites this paper
• 13C Natural Abundance S3E and S3CT Experiments for Measurement ofJCoupling Constants between13Cαor1Hαand Other Protons in a Protein

  1999cites this paper
• NMR Studies of Protein Sidechain Dynamics

  1998cites this paper
• Detection of Nitrogen–NitrogenJ-Couplings in Proteins

  1998cites this paper
• Refined solution structure of the DNA-binding domain of GAL4 and use of 3J(113Cd,1H) in structure determination

  1997cites this paper
• A DQ/ZQ NMR Experiment for the Determination of the Signs of SmallJ(1H,13C) Coupling Constants in Linear Spin Systems

  1997cites this paper
• I-spin n-quantum coherences in InS spin systems employed for E.COSY-type measurement of heteronuclear long-range coupling constants in NMR

  1997cites this paper
• Integration of spin-state-selective excitation into 2D NMR correlation experiments with the heteronuclear ZQ/2Q pi rotations for 1JXH- resolved E.COSY-type measurements of heteronuclear coupling constants in proteins.

  1997cites this paper
• High-resolution solution NMR structure of the Z domain of staphylococcal protein A.

  1997cites this paper
• Measurement of 15N-1H coupling constants in uniformly 15N-labeled proteins: Application to the photoactive yellow protein

  1997cites this paper
• Chapter 8 Use of high power spin-lock purge pulses in high resolution NMR spectroscopy

  1997cites this paper
• Spin-state-selective coherence transfer via intermediate states of two-spin coherence in IS spin systems: Application to E.COSY-type measurement of J coupling constants

  1997cites this paper
• Multidimensional NMR of macromolecules

  1996cites this paper
• Protein Structure Determination from NMR Data

  1996cites this paper
• Simulated annealing with restrained molecular dynamics using a flexible restraint potential: Theory and evaluation with simulated NMR constraints

  1996cites this paper
• NMR investigation of RNA structure

  1996cites this paper
• Measurement of three-bond coupling constants in the osmoregulated periplasmic glucan of Burkholderia solanacearum

  1996cites this paper
• Solving the atomic resolution structure of a protein in solution: nuclear magnetic resonance studies of villin 14T.

  1996cites this paper
• Homonuclear and Heteronuclear Hartmann—Hahn Transfer in Isotropic Liquids

  1996cites this paper
• High-level production of uniformly 15N-and 13C-enriched fusion proteins in Escherichia coli

  1996cites this paper
• Calcium-induced structural changes and domain autonomy in calmodulin

  1995cites this paper
• Determination of heteronuclear three-bond J-coupling constants in peptides by a simple heteronuclear relayed E.COSY experiment

  1995cites this paper
• Novel techniques in nuclear magnetic resonance for nucleic acids.

  1995cites this paper
• Carbon-proton coupling constants in the conformational analysis of sugar molecules.

  1995cites this paper
• Two-, three-, and four-dimensional nuclear magnetic resonance spectroscopy of protein pharmaceuticals.

  1995cites this paper
• Determination of the solution structure of Apo calbindin D9k by NMR spectroscopy.

  1995cites this paper
• (H)NCAHA and (H)CANNH experiments for the determination of vicinal coupling constants related to the ϕ-torsion angle

  1995cites this paper
• Determination of heteronuclear long‐range H,X coupling constants from gradient‐selected HMBC spectra

  1995cites this paper
• SKALARE KOPPLUNGEN : IHRE ANALYSE UND IHRE VERWENDUNG ZUR STRUKTURAUFKLARUNG

  1995cites this paper
• Coupling constants again: Experimental restraints in structure refinement

  1994cites this paper
• Multidimensional NMR Spectroscopy of Peptides

  1994cites this paper
• Calculations of one-, two- and three-bond nuclear spin-spin couplings in a model peptide and correlations with experimental data

  1994cites this paper
• Three-dimensional structure of a type VI turn in a linear peptide in water solution. Evidence for stacking of aromatic rings as a major stabilizing factor.

  1994cites this paper
• Effect of disulfide bridge formation on the NMR spectrum of a protein: Studies on oxidized and reduced Escherichia coli thioredoxin

  1994cites this paper
• 13C-1H Spin-Coupling Constants in Furanosyl Rings: Application to Oligonucleotide Structure Determination

  1994cites this paper
• Isotope labeling in solution protein assignment and structural analysis

  1994cites this paper
• Measurement of long‐range2 13C‐1H coupling constants of 95% uniformly 13C‐labeled polysaccharide from streptococcus mitis J22

  1994cites this paper
• NMR developments in structural studies of carbohydrates and their complexes

  1994cites this paper
• Estimates of ϕ and ψ torsion angles in proteins from one-, two- and three-bond nuclear spin-spin couplings: Application to staphylococcal nuclease

  1994cites this paper
• Measurement of homo- and heteronuclear J couplings from quantitative J correlation.

  1994cites this paper
• Solution structure of human interleukin‐1 receptor antagonist protein

  1994cites this paper
• 13C-1H spin-coupling constants in carbohydrates: magnitude and sign determinations via 2D NMR methods

  1994cites this paper
• Use of chemical shifts and coupling constants in nuclear magnetic resonance structural studies on peptides and proteins.

  1994cites this paper
• Determination of the backbone torsion angle ɛ in nucleic acids

  1994cites this paper
• Modern multidimensional protein NMR spectroscopy. I. Resonance assignment methods

  1994cites this paper
• Modern multi-dimensional protein NMR spectroscopy: II. New experimental approaches

  1994cites this paper
• Refined solution structure of the glucocorticoid receptor DNA-binding domain.

  1994cites this paper
• Measurement of two- and three-bond 13C−1H J couplings to the Cδ carbons of leucine residues in staphylococcal nuclease

  1993cites this paper
• NMR structure-based drug design

  1993cites this paper
• Improved molecular dynamics simulations for the determination of peptide structures

  1993cites this paper
• The use of 1JCαHα coupling constants as a probe for protein backbone conformation

  1993cites this paper
• Measurement of inter-glycosidic 13C-1H coupling constants in a cyclic β(1→2)-glucan by 13C-filtered 2D {1H,1H}ROESY

  1993cites this paper
• Study of Protein Dynamics by NMR

  1993cites this paper
• NMR of proteins.

  1993cites this paper
• The three-dimensional structure of acyl-coenzyme A binding protein from bovine liver: Structural refinement using heteronuclear multidimensional NMR spectroscopy

  1993cites this paper
• Structure of Rapamycin: An NMR and Molecular‐Dynamics Investigation

  1993cites this paper
• Three-dimensional structure of the FK506 binding protein/ascomycin complex in solution by heteronuclear three- and four-dimensional NMR.

  1993cites this paper
• Multidimensional nuclear magnetic resonance methods to probe metal environments in proteins.

  1993cites this paper
• Multidimensional NMR Studies of Immunosuppressant/Immunophilin Complexes

  1993cites this paper
• A general approach for determining scalar coupling constants in polypeptides and proteins

  1992cites this paper
• Changing the inhibitory specificity and function of the proteinase inhibitor eglin c by site-directed mutagenesis: functional and structural investigation.

  1992cites this paper
• Solution structure of the DNA-binding domain of Cd2-GAL4 from S. cerevisiae

  1992cites this paper
• The solution structure of eglin c based on measurements of many NOEs and coupling constants and its comparison with X‐ray structures

  1992cites this paper
• Stereospecific assignments and χ1 rotamers for FKBP when bound to ascomycin from 3 J Hα,Hβ and 3 J N,Hβ coupling constants

  1992cites this paper
• Determination of Hα,Hβ and Hβ,C′ coupling constants in13C-labeled proteins

  1992cites this paper
• Design, synthesis and solution structure of a renin inhibitor Structural constraints from NOE, and homonuclear and heteronuclear coupling constants combined with distance geometry calculations

  1992cites this paper
• Three-dimensional structure in solution of acyl-coenzyme A binding protein from bovine liver.

  1992cites this paper
• Determination of proton-proton coupling constants in 13C-labeled molecules

  1992cites this paper
• A 3D triple-resonance NMR technique for qualitative measurement of carbonyl-Hβ J couplings in isotopically enriched proteins

  1992cites this paper
• Determination of the nuclear magnetic resonance solution structure of the DNA-binding domain (residues 1 to 69) of the 434 repressor and comparison with the X-ray crystal structure.

  1992cites this paper
• 2D and 3D HCCH TOCSY experiments for determining 3J(HαHβ) coupling constants of amino acid residues

  1992cites this paper
• New methods for measurement of long-range proton-carbon coupling constants in oligosaccharides

  1992cites this paper