How the 1D‐NOESY suppresses solvent signal in metabonomics NMR spectroscopy: An examination of the pulse sequence components and evolution

No abstract is available for this paper.

• Publication year

  2011

• Venue

  Concepts in Magnetic Resonance Part A

• Publication date

  2011-09-01

• Fields of study

  Chemistry

• Identifiers
  DOI 10.1002/CMR.A.20223
• External record

  Open on Semantic Scholar

• Source metadata

  Semantic Scholar

• No claims are published for this paper.

• No concepts are published for this paper.

• J-modulation effects in DOSY experiments and their suppression: the Oneshot45 experiment.

  2011cited by this paper
• Solvent signal suppression in NMR.

  2010cited by this paper
• J‐compensated PGSE: an improved NMR diffusion experiment with fewer phase distortions

  2010cited by this paper
• Protein-induced water 1H MR frequency shifts: contributions from magnetic susceptibility and exchange effects.

  2010cited by this paper
• Recent Advances in Solvent Suppression for Solution NMR: A Practical Reference

  2010cited by this paper
• Simultaneous convection compensation and solvent suppression in biomolecular NMR diffusion experiments

  2009cited by this paper
• The Effects of Finite Rectangular Pulses in NMR: Phase and Intensity Distortions for a Spin-1/2

  2009cited by this paper
• Chapter 2 Recent Advances in Solvent Suppression for Solution NMR: A Practical Reference

  2009cited by this paper
• Application of the FLIPSY pulse sequence for increased sensitivity in 1H NMR-based metabolic profiling studies.

  2008cited by this paper
• Solvent suppression using phase-modulated binomial-like sequences and applications to diffusion measurements.

  2008cited by this paper
• Pre-SAT180, a simple and effective method for residual water suppression.

  2008cited by this paper
• PGSTE-WATERGATE: an STE-based PGSE NMR sequence with excellent solvent suppression.

  2008cited by this paper
• Improved residual water suppression: WET180

  2008cited by this paper
• Direct (1)H NMR spectroscopy of dissolved organic matter in natural waters.

  2008cited by this paper
• Single or triple gradients?

  2008cited by this paper
• SOGGY: solvent-optimized double gradient spectroscopy for water suppression. A comparison with some existing techniques.

  2007cited by this paper
• Metabolic profiling, metabolomic and metabonomic procedures for NMR spectroscopy of urine, plasma, serum and tissue extracts

  2007cited by this paper
• Suppression of background gradients in (B0 gradient‐based) NMR diffusion experiments

  2007cited by this paper
• Optimization of NMR analysis of biological fluids for quantitative accuracy

  2006cited by this paper
• Cryogenically cooled probes—a leap in NMR technology

  2005cited by this paper
• Rapid pulse length determination in high-resolution NMR.

  2005cited by this paper
• Purge NMR: effective and easy solvent suppression.

  2005cited by this paper
• Growing pains for metabolomics: the newest 'omic science is producing results--and more data than researchers know what to do with

  2005cited by this paper
• SWET for Secure Water Suppression on Probes with High Quality Factor

  2005cited by this paper
• Convection-compensating PGSE experiment incorporating excitation-sculpting water suppression (CONVEX).

  2004cited by this paper
• A PFG NMR experiment for translational diffusion measurements in low-viscosity solvents containing multiple resonances.

  2004cited by this paper
• Compensation for pulse imperfections in rotational-echo double-resonance NMR by composite pulses and EXORCYCLE.

  2004cited by this paper
• Background gradient suppression in pulsed gradient stimulated echo measurements.

  2003cited by this paper
• Choosing the best pulse sequences, acquisition parameters, postacquisition processing strategies, and probes for natural product structure elucidation by NMR spectroscopy.

  2002cited by this paper
• Recovery of underwater resonances by magnetization transferred NMR spectroscopy (RECUR-NMR).

  2001cited by this paper
• Macroscopic background gradient and radiation damping effects on high-field PGSE NMR diffusion measurements.

  2001cited by this paper
• Radiation damping compensation of selective pulses in water–protein exchange spectroscopy

  2000cited by this paper
• Identification of compounds with binding affinity to proteins via magnetization transfer from bulk water*

  2000cited by this paper
• 90° pulse width calibrations: how to read a pulse width array

  1999cited by this paper
• Suppression of radiation damping in high-resolution NMR.

  1999cited by this paper
• Diffusion Ordered Nuclear Magnetic Resonance Spectroscopy: Principles and Applications

  1999cited by this paper
• Signal selection in high-resolution NMR by pulsed field gradients.

  1999cited by this paper
• Unwanted signal leakage in excitation sculpting with single axis gradients.

  1999cited by this paper
• Water Signal Suppression in NMR Spectroscopy

  1999cited by this paper
• Radiation damping diagnostics

  1999cited by this paper
• Analysis and implications of transition-band signals in high-resolution NMR.

  1998cited by this paper
• Recommendations for the presentation of NMR structures of proteins and nucleic acids – IUPAC-IUBMB-IUPAB Inter-Union Task Group on the Standardization of Data Bases of Protein and Nucleic Acid Structures Determined by NMR Spectroscopy

  1998cited by this paper
• Decoupling: theory and practice II. State of the art: in vivo applications of decoupling

  1997cited by this paper
• Optimization of the water-PRESS pulse sequence and its integration into pulse sequences for studying biological macromolecules.

  1997cited by this paper
• Pulsed-field gradient nuclear magnetic resonance as a tool for studying translational diffusion, part 1: basic theory

  1997cited by this paper
• A pictorial representation of product operator formalism: Nonclassical vector diagrams for multidimensional NMR

  1997cited by this paper
• Suppression of Convection Artifacts in Stimulated-Echo Diffusion Experiments. Double-Stimulated-Echo Experiments

  1997cited by this paper
• Radiation damping effects in solvent preirradiation experiments in NMR

  1996cited by this paper
• Demagnetization field effects in two‐dimensional solution NMR

  1996cited by this paper
• Observation of Bulk Susceptibility Effects in High-Resolution Nuclear Magnetic Resonance

  1996cited by this paper
• Suppression of radiation damping during selective excitation of the water signal: The WANTED sequence

  1996cited by this paper
• Field gradient techniques in NMR spectroscopy.

  1995cited by this paper
• 1H, 13C and 15N chemical shift referencing in biomolecular NMR

  1995cited by this paper
• Improved Accuracy of NMR Structures by a Modified NOESY-HSQC Experiment

  1995cited by this paper
• An Improved Diffusion-Ordered Spectroscopy Experiment Incorporating Bipolar-Gradient Pulses

  1995cited by this paper
• Randomization approach to water suppression in multidimensional NMR using pulsed field gradients.

  1995cited by this paper
• Water Suppression That Works. Excitation Sculpting Using Arbitrary Wave-Forms and Pulsed-Field Gradients

  1995cited by this paper
• Enhanced sensitivity of rapidly exchanging amide protons by improved phase cycling and the constructive use of radiation damping

  1994cited by this paper
• 750 MHz 1H-NMR spectroscopy of human blood plasma.

  1993cited by this paper
• Solvent Suppression by Use of a DANTE Train of B1-Gradient Pulses

  1993cited by this paper
• The Importance of Not Saturating H2o in Protein NMR : application to Sensitivity Enhancement and Noe Measurements

  1993cited by this paper
• Solvent signal suppression in NMR

  1991cited by this paper
• Pulsed field gradient stimulated echo methods for improved NMR diffusion measurements in heterogeneous systems

  1989cited by this paper
• [3] Solvent suppression

  1989cited by this paper
• Fourier transform pulsed-gradient spin-echo studies of molecular diffusion

  1987cited by this paper
• Selective water attenuation by T2 and T1 relaxation in one- and two-dimensional NMR

  1987cited by this paper
• Solvent suppression in Fourier transform nuclear magnetic resonance

  1983cited by this paper
• Efficient detection of paramagnetically shifted NMR resonances by optimizing the WEFT pulse sequence

  1983cited by this paper
• Water and proteins. II. The location and dynamics of water in protein systems and its relation to their stability and properties.

  1983cited by this paper
• Symmetrical composite pulse sequences for NMR population inversion. II. Compensation of resonance offset

  1982cited by this paper
• Symmetrical composite pulse sequences for NMR population inversion. I. Compensation of radiofrequency field inhomogeneity

  1982cited by this paper
• Broadband heteronuclear decoupling

  1982cited by this paper
• The recovery-preparation time in pulsed FT NMR experiments

  1982cited by this paper
• Compensation for Pulse Imperfections in NMR Spin-Echo Experiments

  1981cited by this paper
• A modified pulsed gradient technique for measuring diffusion in the presence of large background gradients

  1980cited by this paper
• A two-dimensional nuclear Overhauser enhancement (2D NOE) experiment for the elucidation of complete proton-proton cross-relaxation networks in biological macromolecules.

  1980cited by this paper
• Water and proteins. I. The significance and structure of water; its interaction with electrolytes and non-electrolytes.

  1978cited by this paper
• Suppression of artifacts in two-dimensional J spectroscopy

  1977cited by this paper
• Water Eliminated Fourier Transform NMR Spectroscopy

  1972cited by this paper
• Some factors in the interpretation of protein denaturation.

  1959cited by this paper
• Radiation Damping in Magnetic Resonance Experiments

  1954cited by this paper

• Multi‐Solvent Suppression Ultrafast 2D COSY for High‐Throughput Wine Screening

  2026cites this paper
• Deamidation and isomerization to elusive isoaspartate in a computationally designed miniprotein

  2026cites this paper
• Effects of Nicotine on SH-SY5Y Cells: An NMR-Based Metabolomic Study

  2025cites this paper
• Antibiofilm activity of a chionodracine-derived peptide by NMR-based metabolomics of cell-free supernatant of Acinetobacter baumannii clinical strains.

  2025cites this paper
• NMR metabolomics in genetically engineered mouse models

  2025cites this paper
• 1H NMR Pure Shift Metabolomic Analysis of Black Tea.

  2025cites this paper
• High-Accuracy Quantitative Nuclear Magnetic Resonance Using Improved Solvent Suppression Schemes

  2025cites this paper
• A Pre-Clinical Study on the Use of the Proprotein Convertase Subtilisin/Kexin Type 9 Inhibitor PEP 2-8 to Mitigate Ischemic Injury in a Rat Marginal Donor Model

  2025cites this paper
• Very First Application of Compact Benchtop NMR Spectrometers to Complex Biofluid Analysis and Metabolite Tracking for Future Metabolomics Studies: A Retrospective Decennial Report from November 2014

  2025cites this paper
• Quantitative Analysis of the Components of Rotigotine Prolonged-Release Microspheres for Injection Using Solvent-Suppressed 1H NMR

  2025cites this paper
• Developments and Applications of Quantitative 1H NMR Methods for Accurate Monitoring of the Human Environments; with Focuses on the Methods for Developing Reference Materials

  2025cites this paper
• Automatic NMR Spectral Profiling of Commercial Cow’s Milk

  2025cites this paper
• Enhanced partial oxidation of methane over a single-atom Cu catalyst using acetonitrile as a cosolvent

  2025cites this paper
• NMR in the age of modern biomedical research and drug discovery.

  2025cites this paper
• Impact of a Formulation Containing Chaga Extract, Coenzyme Q10, and Alpha-Lipoic Acid on Mitochondrial Dysfunction and Oxidative Stress: NMR Metabolomic Insights into Cellular Energy

  2025cites this paper
• Exercise Attenuates Skeletal Muscle Atrophy in Senescent SAMP8 Mice: Metabolic Insights from NMR-Based Metabolomics

  2025cites this paper
• Quantitative Nuclear Magnetic Resonance for Small Biological Molecules in Complex Mixtures: Practical Guidelines and Key Considerations for Non-Specialists

  2025cites this paper
• Current applications of benchtop FT-NMR in food science: From quality control to adulteration detection.

  2025cites this paper
• A machine learning-based nuclear magnetic resonance profiling model to authenticate 'Jerez-Xérès-Sherry' wines.

  2025cites this paper
• Detection of Exchangeable Protons in NMR Metabolomic Analysis Using AI-Designed Water Irradiation Devoid Pulses.

  2025cites this paper
• Disclose ATP-synthase as a protein target of the antimicrobial peptide RiLK1 in Escherichia coli: An alternative receptor-mediated bactericidal mechanism.

  2025cites this paper
• 1H-NMR Analysis of Wine Metabolites: Method Development and Validation

  2025cites this paper
• Impact of a Withania somnifera and Bacopa monnieri Formulation on SH-SY5Y Human Neuroblastoma Cells Metabolism Through NMR Metabolomic

  2024cites this paper
• Automated Beer Analysis by NMR Spectroscopy

  2024cites this paper
• Emerging Contaminants from Bioplastic Pollution in Marine Waters

  2024cites this paper
• Supercritical carbon dioxide likely served as a prebiotic source of methanethiol in primordial ocean hydrothermal systems

  2024cites this paper
• Peptides as modulators of FPPS enzyme: A multifaceted evaluation from the design to the mechanism of action.

  2024cites this paper
• Basic accuracy of a 1D NOESY with presaturation method using standard solutions of amino and maleic acids

  2024cites this paper
• NMR-based plant metabolomics protocols: a step-by-step guide

  2024cites this paper
• Automatic Chemical Profiling of Wine by Proton Nuclear Magnetic Resonance Spectroscopy

  2024cites this paper
• Investigating the Effectiveness of a Carb-Free Oloproteic Diet in Fibromyalgia Treatment

  2024cites this paper
• Understanding the maturity of coconut water through 1H NMR profiling and MPAES analyses.

  2024cites this paper
• Water Suppression 101 for Benchtop NMR– An Accessible Guide and Primer including Fully Interactive Training Videos

  2024cites this paper
• Ultra-clean pure shift NMR with optimal water suppression for analysis of aqueous pharmaceutical samples.

  2024cites this paper
• Twenty Years of 1H NMR Plant Metabolomics: A Way Forward toward Assessment of Plant Metabolites for Constitutive and Inducible Defenses to Biotic Stress.

  2024cites this paper
• Slice through the water-Exploring the fundamental challenge of water suppression for benchtop NMR systems.

  2024cites this paper
• NMR Metabolomics and DNA Sequencing of Escherichia coli and Staphylococcus aureus Cultures Treated with Hydrolyzable Tannins

  2023influential citation
• Exploring the Effects of Probiotic Treatment on Urinary and Serum Metabolic Profiles in Healthy Individuals

  2023cites this paper
• SMN deficiency perturbs monoamine neurotransmitter metabolism in spinal muscular atrophy

  2023cites this paper
• Fingerprinting and profiling in metabolomics of biosamples.

  2023cites this paper
• Spectral and chromatographic analysis of food-related components produced by bacteria, plants, and fungi. A review

  2023cites this paper
• Elucidating the Effect of Amine Charge State on Poly(β-amino ester) Degradation Using Permanently Charged Analogs.

  2023cites this paper
• Applications of Solution NMR Spectroscopy in Quality Assessment and Authentication of Bovine Milk

  2023cites this paper
• Nuclear Magnetic Resonance Study of CO2 Capture by Fluoroalkylamines: Ammonium Ion pKa Depression via Fluorine Modification and Thermochemistry of Carbamylation.

  2023cites this paper
• Detection of barley malt syrup as an adulterant in honey by 1H NMR profile.

  2023cites this paper
• Darjeeling tea profiling using 1H NMR and multivariate analysis

  2023cites this paper
• NMR metabolite quantification of a synthetic urine sample: an inter-laboratory comparison of processing workflows

  2023influential citation
• MagMet: A fully automated web server for targeted nuclear magnetic resonance metabolomics of plasma and serum.

  2023cites this paper
• Automated identification and quantification of metabolites in human fecal extracts by nuclear magnetic resonance spectroscopy.

  2023cites this paper
• Fresh Dual Presaturation Method for Analyzing H2O-Rich Samples Using Quantitative 1H NMR.

  2023cites this paper
• NMR Study of CO2 Capture by Butylamine and Oligopeptide KDDE in Aqueous Solution: Capture Efficiency and Gibbs Free Energy of the Capture Reaction as a Function of pH.

  2023cites this paper
• Elemental sulfur, hydrogen sulfide, and carbon monoxide-driven dimerization of glycine at sub-millimolar concentrations: Implications for the origin of life

  2023cites this paper
• Identifying type of sugar adulterants in honey: Combined application of NMR spectroscopy and supervised machine learning classification

  2022cites this paper
• Nuclear Magnetic Resonance-Based Metabolomics to Predict Early and Late Adverse Outcomes in Ischemic Stroke Treated with Intravenous Thrombolysis

  2022cites this paper
• Study on the Use of Ozone Water as a Chemical Decontamination Agent for Antineoplastic Drugs in Clinical Settings.

  2022cites this paper
• 1H NMR-Based Chemometrics to Gain Insights Into the Bran of Radiation-Induced Colored Wheat Mutant

  2022cites this paper
• Diindolylmethane Promotes Metabolic Crisis and Enhances the Efficacy of Centchroman in Breast Cancer: A 1H NMR-Based Approach

  2022cites this paper
• Grazing affects metabolic pattern of individual cow milk.

  2022cites this paper
• Systematic Review of NMR-Based Metabolomics Practices in Human Disease Research

  2022cites this paper
• NMR spectroscopy as a characterization tool enabling biologics formulation development.

  2022cites this paper
• Nusinersen Induces Disease-Severity-Specific Neurometabolic Effects in Spinal Muscular Atrophy

  2022cites this paper
• Identification of interaction partners using protein aggregation and NMR spectroscopy

  2022cites this paper
• Development, Validation, and Use of 1H-NMR Spectroscopy for Evaluating the Quality of Acerola-Based Food Supplements and Quantifying Ascorbic Acid

  2022cites this paper
• NMR-Based Metabolomics in Differential Diagnosis of Chronic Kidney Disease (CKD) Subtypes

  2022cites this paper
• Metabolomics Fingerprint Predicts Risk of Death in Dilated Cardiomyopathy and Heart Failure

  2022cites this paper
• Updates and Original Case Studies Focused on the NMR-Linked Metabolomics Analysis of Human Oral Fluids Part I: Emerging Platforms and Perspectives

  2022cites this paper
• Metabolite Biomarkers of Leishmania Antimony Resistance

  2021cites this paper
• Comparison of Regular, Pure Shift, and Fast 2D NMR Experiments for Determination of the Geographical Origin of Walnuts

  2021cites this paper
• Automatic 1D 1H NMR Metabolite Quantification for Bioreactor Monitoring

  2021cites this paper
• Precision Oncology via NMR-Based Metabolomics: A Review on Breast Cancer

  2021cites this paper
• Enhanced characterization of yeast hydrolysate combining acid digestion and 1D‐1H NMR targeted profiling

  2021cites this paper
• Recent advances in benchtop NMR spectroscopy and its applications

  2021cites this paper
• Mitochondrial Regulation Assessment by 13C-NMR Isotopomer Analysis.

  2021cites this paper
• Detection of Metabolite-Protein Interactions in Complex Biological Samples by High-Resolution Relaxometry: Toward Interactomics by NMR.

  2021cites this paper
• Principal Component Analysis of 1D ¹H Diffusion Edited NMR Spectra of Protein Therapeutics.

  2021cites this paper
• Personalized Metabolic Profile by Synergic Use of NMR and HRMS

  2021cites this paper
• Pharmacometabolomics by NMR in Oncology: A Systematic Review

  2021cites this paper
• Degradation and inactivation efficacy of ozone water for antineoplastic drugs in hospital settings

  2021cites this paper
• Aqueous Metabolite Trends for the Progression of Nonalcoholic Fatty Liver Disease in Female Bariatric Surgery Patients by Targeted 1H-NMR Metabolomics

  2021cites this paper
• An ensemble approach to the structure-function problem in microbial communities

  2021cites this paper
• Evaluation of ORAC, IR and NMR metabolomics for predicting ripening stage and variety in melon (Cucumis melo L.).

  2021cites this paper
• The impact of reductants on the catalytic efficiency of a lytic polysaccharide monooxygenase and the special role of dehydroascorbic acid

  2021cites this paper
• Automatic 1D 1 H NMR Metabolite Quantification for Bioreactor Monitoring

  2021cites this paper
• 1H Nuclear Magnetic Resonance Spectroscopy-Based Methods for the Quantification of Proteins in Urine.

  2021cites this paper
• SMolESY: an efficient and quantitative alternative to on-instrument macromolecular 1H-NMR signal suppression†

  2020cites this paper
• Magnetic resonance spectroscopy for the study of cns malignancies

  2020cites this paper
• Quantitative NMR-Based Biomedical Metabolomics: Current Status and Applications

  2020cites this paper
• NMR-based metabolomic profile of hypercholesterolemic human sera: Relationship with in vitro gene expression?

  2020influential citation
• Mechanistic study on the conversion of d-fructose into deoxyfructosazine: Insights from NMR and DFT study

  2020cites this paper
• Use of NMR for the Analysis and Quantification of the Sugar Composition in Fresh and Store-Bought Fruit Juices

  2020cites this paper
• Gradient-based pulse sequences for benchtop NMR spectroscopy.

  2020cites this paper
• Strategy for improved characterization of human metabolic phenotypes using a COmbined Multi-block Principal components Analysis with Statistical Spectroscopy (COMPASS)

  2020cites this paper
• Development of a food class-discrimination system by non-targeted NMR analyses using different magnetic field strengths.

  2020cites this paper
• NMR-based analysis of pomegranate juice using untargeted metabolomics coupled with nested and quantitative approaches.

  2020cites this paper
• Plasma metabolome and cognitive skills in Down syndrome

  2020cites this paper
• 1D and 2D NMR spectra of coffee from 27 countries

  2020cites this paper
• NMR-based metabolic profiling to follow the production of anti-phytopathogenic compounds in the culture of the marine strain Streptomyces sp. PNM-9.

  2020cites this paper
• Diauxie and co-utilization of carbon sources can coexist during bacterial growth in nutritionally complex environments

  2020cites this paper
• A community-built calibration system: The case study of quantification of metabolites in grape juice by qNMR spectroscopy.

  2020cites this paper
• Prenatal and Early Postnatal Cerebral d-Aspartate Depletion Influences l-Amino Acid Pathways, Bioenergetic processes, and Developmental Brain Metabolism.

  2020cites this paper